页岩油储层前置CO2压裂液滤失规律与控制方法实验研究

Experimental study on filtration behavior and control methods of pre-pad CO2 fracturing fluids in shale oil reservoirs

  • 摘要: 为探究适用于页岩储层的新型二氧化碳压裂液体系的滤失行为及其控制机制,选取胜利油田某区块的天然页岩岩心,通过高压动态滤失实验系统,在模拟地层条件下开展了系统对比实验,旨在为页岩储层高效压裂技术及碳捕集、利用与封存(CCUS)中CO2注入策略提供理论指导。分析了单相CO2渗流过程中温度、压力、增稠剂浓度及地层原油对其滤失行为的影响机制,并重点研究了超临界状态下CO2在不同温压条件下的动态滤失特性。通过计算滤失系数,揭示了温压条件对液态CO2在页岩中滤失行为的作用规律。研究结果表明,当CO2处于单相渗流状态时,黏度是控制滤失速率的关键因素:随温度升高或压力降低,CO2黏度下降,滤失系数增大。向CO2中添加增稠剂可有效减缓滤失速度,与纯CO2相比其滤失系数降低约一个数量级。地层原油通过形成气液两相流和附加渗流阻力进一步抑制滤失。当地层中的CO2由液相转变为超临界状态时,两相流效应和体积膨胀作用成为影响滤失速率的主导机制,有效控制滤失速率。超临界状态下,滤失系数随地层温度升高或压力降低而减小或趋于稳定。研究明确了CO2压裂液体系在页岩中的动态滤失规律,可为页岩储层CO2高效压裂技术的优化设计提供重要数据支撑。

     

    Abstract: To investigate the filtration behavior and control mechanisms of novel carbon dioxide (CO2) fracturingfluid systems suitable for shale reservoirs, systematic comparative experiments were conducted under simulated formation conditions using natural shale cores from a block of Shengli Oilfield with a high-pressure dynamic filtration experimental system, aiming to provide theoretical guidance for efficient fracturing technology in shale reservoirs and CO2 injection strategies in carbon capture, utilization, and storage (CCUS). The influencing mechanisms of temperature, pressure, thickener concentration, and formation crude oil on the filtration behavior during single-phase CO2 flow were analyzed, with particular focus on investigating the dynamic filtration characteristics of CO2 under different temperatures and pressures in the supercritical state. The filtration coefficient was calculated to reveal the effects of temperatures and pressures on the filtration behavior of liquid CO2 in shale. The results showed that when CO2 was in a single-phase flow state, viscosity was the key factor controlling the filtration rate. As temperature increased or pressure decreased, the viscosity of CO2 decreased, leading to an increase in the filtration coefficient. The addition of thickeners to CO2 could effectively reduce the filtration rate, with the filtration coefficient decreased by approximately one order of magnitude compared with pure CO2. The presence of formation crude oil further inhibited filtration by forming gas-liquid two-phase flow and additional flow resistance. When CO2 transitioned from liquid phase to supercritical state in the formation, two-phase flow effects and volume expansion became the dominant mechanisms affecting filtration rate, effectively controlling the filtration rate. In the supercritical state, the filtration coefficient decreased or tended to stabilize as formation temperature increased or pressure decreased. This study clarifies the dynamic filtration patterns of CO2 fracturing fluid systems in shale, and it provides important data support for the optimized design of efficient CO2 fracturing technology in shale reservoirs.

     

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